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Characterization of Porcelain Raw Material
This STA measurement on porcelain raw material shows three mass-loss steps. Below approx. 250°C, the evaporation of humidity occurred. At temperatures between 250°C and 450°C, the burn-up of organic content was observed, during which 156 J/g of energy was released. The dehydration of kaolin occurred above 450°C and required 262 J/g. The mass spectrometer signals for mass numbers 18 and 44 reflect the corresponding release of H2O and CO2. The exothermic DSC peak at 1006°C with an enthalpy of -56 J/g is due to an solid-solid transition.

Building Material: Glass Wool
Glass Wool is often used for the insulation of houses and heating pipes. The STA measurement shows three mass-loss steps below approx. 600°C, which are due to the evaporation of humidity and the burn-up of organic binder. The latter can be seen from the strongly exothermic DSC signal in this temperature range. The step in the DSC signal at 728°C with an increase in the specific heat of 0.41 J/(g*K) is due to the glass transition. The exothermic DSC peak at 950°C with an enthalpy of -287 J/g is due to crystallization; the endothermic effects between approx. 1050°C and 1250°C with an entire enthalpy of 549 J/g show the melting. The slight mass changes above 700°C are most probably due to oxidation and evaporation of impurities.

 

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FTIR Coupling

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NETZSCH offers instruments for thermal analysis, thermal properties measurement, thermal hazard screening, and contract testing services. Our portfolio is the world's broadest, including a full range of dilatometers to measure high accuracy thermal expansion, classical DSC & TGA, high temperature DSC to 1650°C for specific heat, very high temperature STA (TGA-DSC/DTA) from sub-ambient to 2400°, thermal / evolved gas analysis with fully-integrated FTIR & MS, high resolution TMA and DMA, plus DEA - dielectric analysis for thermoset cure monitoring. We also feature leading-edge technology for thermal conductivity by guarded hot plate and heat flow meters, laser flash thermal diffusivity measurement, thermal hazard screening via adiabatic reaction calorimetry, as well as refractories testing including HMOR, CIC, and RUL. Finally, we offer advanced software packages including thermokinetics for process modeling and development.

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Last update: 04/22/2009 , Copyright © 2000-2006 NETZSCH-Geraetebau GmbH